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- What is the relationsiip 2) Give the systematic name of the adduct formed when maleic anhydride reacts with 1,3-butadiene. 3) How many signals are in the HNMR spectrum of a. trans-1,2-dibenzoyllethylene b. cis-1,2-dibenzoyllethylene c) How do they differ? AG in l/mol for this d) Name the magnetic effect operating that accounts for their difference 4) Draw the correct structures for the following: phenol nitronium cation meta-nitr O = N= D para- nitrophenolWhich one of the following statements about arene oxides is FALSE? O The NIH shift is what makes arene oxides carcinogenic. O Ring opening of an arene oxide can afford an addition product and/or a rearranged product. O Large polycyclic aromatic hydrocarbons such as benzo[a]pyrene are especially susceptible to arene oxide formation. The NIH shift mechanism was discovered at the National Institutes of Health. O Cytochrome P450 is the powerful biological oxidant that epoxides an arene to give an arene oxide.(R)-Pulegone is converted to (R)-citronellic acid by addition of HCI followed by treatment with NaOH. CI 1. NAOH 2. HCI HCI HO (R)-Pulegone (R)-Citronellic acid Propose a mechanism for each step in this transformation and account for the regiose- lectivity of HCI addition.
- But-2-yne has a pK.~ 38. Evaluate the ability of bases to deprotonate the provided acid.Treatment of acetylene with a suitable base affords lithium acetylide, which was used as a reagent in a partial synthesis of the antitumor natural product (+)-acutiphycin. (Org. Lett. 2014, 16, 1168-1171) Possible bases to consider H-C=C-H Acetylene Step 1 Li :Base T H-O: Li Lithium hydroxide (LiOH) three steps Lithium acetylide Draw the structure of lithium acetylide. Draw Your Solution di. Η Η Η Η | | | | H-C-C-C-C: II HH HH Butyllithium (BuLi) OR CEC- Li OH CH3 -H CH3 Lithium diisopropyl amide (LDA) OMe H3C H H₂C many steps Li HO OH I (+)-Acutiphycin CH3 CH₂ "OHthe correct answer is 5-sulfanylhept-3-yn-2-one and N-ethyl-N,3-dimethylbutanamide respectively. why is your given answer wrong? please give explanation and recheck.
- Draw the structure of the organobromide that can be used to prepare the following Gilman reagent. • You do not have to consider stereochemistry. • You do not have to explicitly draw H atoms. 0-> / -CH₂ CuLi *** Y Sn [1* 4²Which set of reagents would be appropriate to synthesize bromobenzene from benzene? 1. HNO3 in H2SO4; 2. H2Cr04 and heat 1. H2CrO4 and heat; 2. H2 Pd/C Br2 and FeBr3 1. CH3CH2CHCI and AICI3; 2. H204 and heat 4B12 and Fe Heat and Br2 Br2, HCIWrite the expected product for each of the following reactions: Diphenyl sulfide + 1 eq. NaOCl -------------> ? 1,2-Epoxy-3,3-dimethylbutane + 1 eq. CH3CH2SNa then CH3Br -------------> ? 1,2-Epoxy-3-phenylpropane + HCl ------------> ?
- Cc.5. Draw the mechanism of the Beckmann rearrangement of oxime from 4'-bromoacetophenone with hydroxylamine HCl, sodium acetate trihydrate with polyphosphoric acidGive the reason(s) of the following statements: 1. t-Butyl > isopropyl > ethyl > methyl for relative migratory aptitude in Wagner-Meerwein rearrangement 2. The pinacol rearrangement takes place under acidic conditions. 3. Phenyl group move fast in this reaction: H H2SO4 H. Н. A ОнWhich of the following reagents would carry out the isotopic substitution reaction shown below? 16 18 НАС CH3 Н С "CHЗ Cr1803/pyridine O H2180/HCI (cat.) O 1802/Ni (cat.) 1803