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Titration Lab

Decent Essays

Titration can be used to standardize a solution. In this experiment, sodium hydroxide was used to titrate KHP solution. Using the results of the titration, the exact concentration of NaOH was calculated to three significant figures. As see in data table A.1, the volume of NaOH used in trial one is 25.95 mL, and moles of KHP is 0.003501 mol. Using this information, the molarity of NaOH was found by using the formula, Mass of sample x (1 mole/ atomic mass), in Table A.2. After plugging in the appropriate values and taking the average of the three trials, the molarity of NaOH is calculated to be 0.136 M. The calculated molarity has three sig-figs, which is more exact than the 0.1M solution that was provided. Therefore, the data supports the conclusion …show more content…

To begin with, the unknown acid did not dissolve in the water completely. At first, this problem caused the titration to be messed up. Next, a new trail was done by letting the acid settle to the bottom, then taking the solution of without including any precipitate from the bottom of the beaker. In addition, when the unknown acid dissolved in the water, a foggy solution was created. This caused the titration to be tricky because it made it difficult to notice the change of color. Finally, the NaOH that was used at first used in part B did not change color when it was added with the indicator. This happened because the NaOH solution was prepared two weeks prior to this part of the lab. The NaOH might have changed its properties as time went on, for instance, its concentration might have changed. This problem was fixed by making a new NaOH solution. Other than that, everything worked properly. However, one problem that might have occurred was overshooting the solution. This could have been done by adding a large volume of the titrant to the solution, which causes the pH of the solution to be messed up. Another problem that might have occurred was using contaminated lab equipment. This problem would cause a base or an acid to change their pH leading to errors during the lab. However, this problem was prevented by rinsing all glassware with deionized

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