To perform module 9 analysis, we followed Lab safety procedure by wearing safety goggles (Z87 brand), plastic apron, and a pair of latex gloves as a proper “PPE”. The team proceeded to gather module 9 analysis equipment which consisted of; an Oakton PCS tester 35 series, a HACH HQ40d portable multi-meter, a HACH digital titrator with Sodium thiosulfate titration cartridge 0.200 N, and delivery G tube. Furthermore, a stand ring with universal clamp, magnetic stirrer with magnetic stir bar, 1 Plastic Graduated cylinder (100 ml), 2 Plastic sample containers (250 ml), 2 Glass BOD Bottle (300 ml) with stopper, dissolved oxygen reagent powder pillows (2 Manganous Sulfate, 2 Alkaline Iodide-Azide,2 Sulfamic Acid powder pillows), and nail clipper. 1 Erlenmeyer flask (250 ml), Buffer standard solution for pH (4.0, 7.0, and 10.0) and Conductivity (12880µS), starch indicator solution, DI water bottle, Kim wipes. Upon gathering, we set the Lab data sheet, COC sheet, pencil, and calculator.
We draw a sample solution from the churn splitter (after thoroughly mixed) into a (250 ml) plastic sample container and closed the lid. Rinsed Oakton meter with DI water. Set the meter for pH (USA) unit and calibrated with a pH buffer standard solution (4.0. 7.0, 10.0), followed by rinsing with DI water. The meter soaked into plastic sample container and measured the pH, at the same time took the temperature reading in (F°) and TDS reading in (PPM) of the sample, followed by rinsing with DI water.
This document is not meant to be a substitute for a formal laboratory report. The Lab Report Assistant is simply a summary of the experiment’s questions, diagrams if needed, and data tables that should be addressed in a formal lab report. The intent is to facilitate students’ writing of lab reports by providing this information in an editable file which can be sent to an instructor.
1. We measured 2 mL of diluted hydrogen peroxide (the substrate), 1 mL of guaiacol (the product indicator), and 1 mL of neutral buffer (pH 7) with a syringe and disposed it into tubes 1, 2 , 4, 9, 11, and 12.
This document is not meant to be a substitute for a formal laboratory report. The Lab Report Assistant is simply a summary of the experiment’s questions, diagrams if needed, and data tables that should be addressed in a formal lab report. The intent is to facilitate students’ writing of lab reports by providing this information in an editable file which can be sent to an instructor.
Prepare standard solution #1, Take 1 ml sub stock solution from the 100 ml beaker and then put into 25 ml volumetric flask with the help of 10ml graduate pipette.
This document is not meant to be a substitute for a formal laboratory report. The Lab Report Assistant is simply a summary of the experiment’s questions, diagrams if needed, and data tables that should be addressed in a formal lab report. The intent is to facilitate students’ writing of lab reports by providing this information in an editable file which can be sent to an instructor.
In a third test tube, put 1 mL of chutney. Repeat steps 2 and 3 with the chutney and record the results in Table 3.
No credit will be given for this lab report if the Data section is not completely filled out and if the required photographs are not received. At least one photograph must show the student’s face.
This document is not meant to be a substitute for a formal laboratory report. The Lab Report Assistant is simply a summary of the experiment’s questions, diagrams if needed, and data tables that should be addressed in a formal lab report. The intent is to facilitate students’ writing of lab reports by providing this information in an editable file which can be sent to an instructor.
Note: Your prelab/lab report is to be done in your carbon copy lab notebook (sold in FIU bookstore)
Prescription safety glasses are the answer for anyone who wears prescription glasses and requires safety glasses. However, finding the right prescription safety glasses can be a bit of a challenge. Most optometrists don't stock this type of protective eyewear. Many online sites offer prescription safety glasses. However, the key here is to make sure that you are purchasing from a reputable safety glass providers.
There are many hazards in different scientific environments, in this assessment the Jack Hunt School Science Laboratory, the Peterborough Power Station and the Jack Hunt School Kitchens will be the different scientific environments observed. The hazards in each environment, the safety legislation that is put in place to prevent danger as well as other safety measures that are taken by those who work in these environments will be explained.
* Temperature * Method of measuring solutions I will use equal amounts of trypsin, milk, PH, buffer and distilled water in all the experiments and will use the same measuring equipment to ensure fair representation of the effect of different PH on digestion.
First, three titration curves and three second derivative curves were created to determine the average pH at the half-equivalence point from the acetic acid titrations. Titration curves were used as visuals to portray buffer capacity. The graphs and a table, Table 1, that showcased the values collected were created and included below. The flat region, the middle part, of Figures 1, 2 and 3, showed the zone at which the addition of a base or acid did not cause changes in pH. Once surpassed, the pH increased rapidly when a small amount of base, NaOH, was added to the buffer solution. Using the figures below and
12. The crocodile clips are attached to the copper electrodes of the experimental apparatus and the power supply is turned on. Simultaneously, the stopclock is started. The thermometer is checked every 30s. 13. After 300s the stopclock is stopped and the power supply is turned off. The negative cathode is carefully removed and is dried using a hair dryer. 14. When dry the negative cathode is placed on the electronic milligram balance and its final mass is recorded. 15. The positive anode and negative anode of the experimental apparatus are disposed and the electrolyte is poured out to ensure that the anode slime (impurities) does not contaminate the solution. 16. The electrodes of the experimental apparatus are replaced with new copper strips. 17. Steps 7 to 16 are repeated. However, this time, the rheostat is adjusted using the calibration apparatus until the multimeter shows approximate readings of 0.40 A, 0.60 A, 0.80 A and 1.00 A respectively. 18. Time permitting, the entire experiment is repeated. Safety Copper sulphate may cause irritation and burns if it comes into contact with the eyes. As standard lab procedure, safety goggles and lab coats must be worn at all times. Control of Variables Volume of Electrolyte Used
For this experiment, a pH meter was used so this part of the experiment began with the calibration of the pH meter with specified buffers. The buret was then filled with the standard HCl solution and a set-up for titration was prepared. 200g of the carbonate-bicarbonate solid sample was weighed and dissolved in 100 mL of distilled water. The sample solution was then transferred into a 250-ml volumetric flask and was diluted to the 250-mL mark. The flask was inverted several times for uniform mixing. A 50-mL aliquot of the sample solution was measured and placed unto a beaker. 3 drops of the phenolphthalein indicator was added to the solution in the beaker. The electrode of the pH meter was then immersed in the beaker and the solution containing the carbonate-bicarbonate mixture was titrated with the standard HCl solution to the phenolphthalein endpoint. Readings of the pH were taken at an interval of 0.5 mL addition of the titrant. After the first endpoint is obtained, 3 drops of the methyl orange was added to the same solution and was titrated with the standard acid until the formation of an orange-colored solution. Readings of the pH were also taken at 0.5 mL addition of the titrant.