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Aluminum Foil Lab Report

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Feasibility Study of Producing Potassium Alum via Aluminum Foil Lujia Cheng and Shalin Presgraves CHEM 1065, Experiment No.5, October 11, 2016 Abstract. Alum is one of the oldest and the most explored substance in human history. Dozens of ways were discovered to produce it. One way of synthesizing potassium alum was covered in this report. In this synthesis, aluminum foil, an everyday material, was the reactant. This synthesis includes two main steps. First, dissolves aluminum in potassium hydroxide. Second, treat it with sulfuric acid and filter out the product. This synthesis was found out to be an efficient way to produce small amount of potassium alum under a laboratorial environment. Introduction. Alum can be specific to one compound, …show more content…

It was used in ancient China as a medicine while in Europe as a mordant for dyes. Yet, alum still has it place in modern age, like clarifying water.1 Aluminum is also known as its reactivity. Due to that, its element form was barely found in nature. However, in this synthesis method, pure aluminum was used as a reactant. This would suggest that this method was not suitable for mass production potassium alum. Even though pure aluminum cannot be found in nature, but it is widely appears in daily life, for example, the oven-used aluminum foil or gum wrapper. As a result, this method fits in our daily life to produce small amount of potassium alum instead of mass-producing. This synthesis can break down into two specific steps. Each steps was illustrated by the reactions, equation (1) and equation (2). As them indicate, the first step is to use hot potassium hydroxide to dissolve aluminum foil. The second step is to add potassium hydroxide which results potassium …show more content…

Aluminum foils (0.48 g in total) was weighted and dissolved into boiled KOH (20 ± 0.02 mL) solution. As soon as the foil touched the hot KOH, bubbles appeared on the surface of the foil and the solution turned into a black suspension. After fully reacted, vacuum filtrate, the suspension separated to black residue and transparent filtrate. Residue was discarded and the acidity (pH = 9) of solution was measured at this time. Slowly adding sulfuric acid (about 5 mL of 9M) into the solution, white precipitate appeared. When most precipitate appeared, acid (1.4 ± 0.06 mL) was added. Acidity (pH = 8) was measured again and the reaction liberated a lot of heat. After all the acid was added, the precipitate mostly dissolved. All precipitate dissolved after heating. Acidity was measured again (pH = 3.5). Ice bath (10 minutes) and evoked crystallization. After crystallized fully, vacuum filtrate (5 minutes) the crystal-liquid mixture. Residue, white powder, was rinse by cold ethanol and collected. A few milligrams of crystals were transferred to a tube for a spot test. The crystal dissolved into water with ease. However, it turned milky white when sodium bicarbonate was

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