The calcium content of a urine specimen was determined by using an ion selective electrode. The following values were obtained: 102, 97, 99, 98, 101, 106 mM. What are the 95% confidence limits for the calcium concentration?
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- A student performed a titration to determine the exact concentration of NaOH(aq). The titration was performed against a standard 0.1000 M HCl(aq) solution. Phenolphthalein indicator was used. The following end-point volumes were recorded by the student in units mL: Trial Number Volume 1 25.06 2 25.15 3 25.02 4 25.17 5 25.07 Calculate the 95% confidence limit. Assume that there is no outlier. Provide your answer to the correct number of decimal places, without units, and without the ± sign. Use the T-table shown below.You were assigned to assay a product sample of milk of magnesia. A 0.600-g sample was reacted with 25.00 mL 0.10590 N H2SO4 . The excess unreacted acid in the solution required 13.00 mL of 0.09500 N NaOH when titrated to reach the methyl red end point. Determine the dosage strength of the product in terms of % Mg(OH)2 content. Type your answer in 2 decimal places, numbers only.A researcher reconstituted a vial of 750 mg Cefuroxime Sodium Powder for Injection with 6mL of sterile water for injection. The reconstituted solution was dark amber-colored solution. The package insert states that solution colors range from clear to yellow depending on concentration, diluent, and storage conditions. The researcher was then hesitant to give the patient the solution due to its unusual dark color. Five portions were taken from a batch of cefuroxime sodium. Prior to testing in the instrument, each part was subjected to one of the following conditions: Conditions Specifications Temperature Portion 1: 8°C ± 2°C Portion 2: 30°C ± 2°C Portion 3: 40°C ± 2°C Light Portion 4: Kept in the dark Portion 5: Exposed to direct sunlight 1. Of the several solutions prepared, which absorbance value results should be compared with each other to answer the questions of the pharmacist? Explain your answer.
- One of the CHEM3341 student Ms. Fatima Al Wahaibi wanted to analyse phosphate ion concentration in Fertilizer industry wastewater sample collected from Rusayl Industrial Estate using spectrophotometer method. She mixed 200.00 mL of wastewater sample which contains only Na;PO, (unknown molarity) with 400.00 mL of 0.0200 M K,PO4 in a one liter beaker to make a Solution A. She then transferred 25.00 mL of Solution A to a 250.00 mL volumetric flask and added distilled water up to the calibration mark to make up Solution B. The Concentration of phosphate ions in Solution B is known to contain 3.00 x 103 mol/L from the spectrophotometric analysis at 460 nm using 1 cm cuvette. Calculate the concentration of phosphate ion in wastewater and how many phosphate ions are present in this wastewater.The Kjeldahl method was used to determine the nitrogen content of a protein. A 275 µL aliquot of a 47.0 mg/mL protein solution was digested in boiling sulfuric acid. The solution was made basic and the liberated NH, was collected in 5.00 mL of 0.0512 M HCl. A volume of 7.00 mL of 0.0174 M NaOH was required to react with the excess HCl. Calculate the weight percent of nitrogen in the protein. weight percent: wt% NThe table below describes a procedure in preparing standard solutions of a protein sample with different concentrations. (A) Determine the concentrations of each tube if the starting concentration of the protein is 500 mg mL (B) Determine the equation of the line if the concentration (x-axis) was plotted vs the absorbance (y-axis). (C) What is the concentration, in mg mL, of the diluted unknown protein sample if the absorbance at 595 nm is 0.333? L-1. Tube Volume of protein, Volume of water, Final concentration, Absorbance #3 mL mL (at 595 nm) mg mL-1 0.00 5.00 0.113 12 0.70 4.30 0.184 3 1.40 3.60 0.251 14 2.10 2.90 0.329 15 2.80 2.20 0.385 3.50 1.50 0.454 17 4.20 0.80 0.503 8 5.00 0.00 0.577 Suppose that the unknown protein (diluted) sample in 4.C was diluted from a protein stock solution. Determine the concentration of the original unknown protein stock solution if 2.00 mL of the protein solution was mixed with 8.00 mL of water to create the unknown protein (diluted) sample in 4.C.
- You took 25.00 mL of unknown water solution and titrated it with EDTA. The EDTA solution molarity was 0.01 M, and it took 16.50 mL to reach the end point. With the blank it took only 0.98 mL to reach end point. 15.52 mL of EDTA solution were used to titrate hardness that actually came from the unknown 1.552×10−4 moles of EDTA reacted with hardness-causing ions from the unknown sample 1.552×10−4 moles of hardness-causing ions were present in the unknown sample A) Assuming that the total hardness of water is due to CaCO3, how many grams CaCO3 does it correspond to? B) What is the total hardness of the unknown water in ppm CaCO3?WARIARTAM 2. 1.2589 g of a certain brand of milk powder required 25.89 mL of 0.01873M EDTA to titrate the calcium contained in the sample. (a) What is the percent calcium in the sample? (b) Would the true result be higher, lower, or not be affected if the milk powder sample has been slightly wet?A 1.407 g sample of canned tuna was analyzed by the Kjeldahl method. The liberated NH3 required 26.45 mL of 0.1180 M HCl. Calculate the percentage nitrogen and protein in the sample. Assume that the protein factor is 6.25, i.e. % protein = % N x 6.25.
- 2+ as (6) A sample of an ore was analyzed for Cu* follows. A 1.25 g sample of the ore was dissolved in acid and diluted to volume in a 250 mL volumetric flask. A 20 mL portion of the resulting solution was transferred by pipet to a 50 ml volumetric flask and diluted to volume. An analysis showed that the concentration of 2+ Cu* in the final solution was 4.62 ppm. What is the weight percent of Cu in the original ore?Five white, 500-mg uncoated ascorbic acid (AA) tablets with an average weight of 0.6152-g were pulverized in a mortar. A sample of the powdered ascorbic acid weighing 0.4700-g was placed in an iodine flask and was dissolved in 50-mL H2SO4 then 5-g of KBr was added to the resulting solution. The solution was titrated with 47.81-mL of 0.09640 N STD. KBrO3 to reach a faint yellow endpoint then 3-g KI and 5-mL Starch TS. The blue color solution is then titrated with 2.73-mL of 0.09123 N STD. Na2S2O3 to reach the disappearance of the blue iodostarch complex. MW: KBrO3 = 167.0 ; KIO3 = 214.0 ; Na2S2O3 = 158.11 ; C6H8O6 = 176.12 Compute the milligrams of pure AA per tablet from the assay. 293.3 mg 502.5 mg None of the choices 383.9 mgExample You determine the acetic acid content in vinegar by titrating with a standard (known concentration) solution of NaOH to a phenolphthalein endpoint. 5.023± 0.003 g sample of vinegar is weighed. The NaOH must be standardized by KHP and 3 such titrations gave molarities of 0.1167, 0.1163 and 0.1164 M. A volume of 36.78 ± 0.03mL NaOH is used to titrate the sample. What is the percent acetic acid in the vinegar and what is the overall uncertainty?Answer: 5.12% ± 0.01%