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If the Product of this Suzuki reaction is 4-(4-methylphenyl)benzaldehyde, what are the two starting reagents?

If the Product of this Suzuki reaction is 4-(4-methylphenyl)benzaldehyde, what are the two starting reagents?

Introduction to General, Organic and Biochemistry
Introduction to General, Organic and Biochemistry
11th Edition
ISBN:9781285869759
Author:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres
Publisher:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres
Chapter14: Alcohols, Ethers, And Thiols
Section: Chapter Questions
Problem 14.48P: 14-48 Explain why methanethiol, CH3SH, has a lower boiling point (6°C) than methanol, CH3OH (65°C),...
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If the Product of this Suzuki reaction is 4-(4-methylphenyl)benzaldehyde, what are the two starting reagents?

4(4'-methylphenyl)-benzaldehyde 107 °C10 H
Transcribed Image Text:4(4'-methylphenyl)-benzaldehyde 107 °C10 H
Suzuki Cross Coupling Reaction Synthesis of an Unsymmetrical Biaryl via a Suzuki Cross Coupling Reaction' Experimental Goals: Perform the cross coupling reaction from two unknown coupling partners and isolate the product. Determine the structure of the product from its IR and NMR spectra and melting point, and in tum determine the starting materials. B(OH)2 Pd(OAc)2, PPH3 аq NazCOs Br R' n-PrOH R = H, CH3 R' = H, CH3, OCH3 R" Name Structure mp 1-biphenyl-4-yl-ethanone 120-121°C* CHS 1-biphenyl-4-yl-ethanol 96-98 °C CH3 biphenyl-4-carbaldehyde 60-63 "C OH 4-phenyl-benzyl alcohol 104-105 °C" H. 1-(4"-methyl-biphenyl-4-yl) ethanone 119-120 °C CH3 OH 1-(4'methyl-biphenyl-4-yl)-ethanol 95-96 "C" CH3 4(4'-methylphenyl)-benzaldehyde 107 °C" он 4'-methyl-(biphenyl-4-yl)-methanol 100-101 "C H. 1-(4"-methoxy-biphenyl-4-yl)-ethanone Meo 153-154 "C2 CH3 OH 1-(4'-methoxy-biphenyl-4-yl)-ethanol Meo 120-122 °C CH3 4'-methoxy-biphenyl-4-carbaldehyde Meo 105-106 "C4 H. OH 4'-methoxy-biphenyl-4-yl-methanol 162-163 "C Meo
Transcribed Image Text:Suzuki Cross Coupling Reaction Synthesis of an Unsymmetrical Biaryl via a Suzuki Cross Coupling Reaction' Experimental Goals: Perform the cross coupling reaction from two unknown coupling partners and isolate the product. Determine the structure of the product from its IR and NMR spectra and melting point, and in tum determine the starting materials. B(OH)2 Pd(OAc)2, PPH3 аq NazCOs Br R' n-PrOH R = H, CH3 R' = H, CH3, OCH3 R" Name Structure mp 1-biphenyl-4-yl-ethanone 120-121°C* CHS 1-biphenyl-4-yl-ethanol 96-98 °C CH3 biphenyl-4-carbaldehyde 60-63 "C OH 4-phenyl-benzyl alcohol 104-105 °C" H. 1-(4"-methyl-biphenyl-4-yl) ethanone 119-120 °C CH3 OH 1-(4'methyl-biphenyl-4-yl)-ethanol 95-96 "C" CH3 4(4'-methylphenyl)-benzaldehyde 107 °C" он 4'-methyl-(biphenyl-4-yl)-methanol 100-101 "C H. 1-(4"-methoxy-biphenyl-4-yl)-ethanone Meo 153-154 "C2 CH3 OH 1-(4'-methoxy-biphenyl-4-yl)-ethanol Meo 120-122 °C CH3 4'-methoxy-biphenyl-4-carbaldehyde Meo 105-106 "C4 H. OH 4'-methoxy-biphenyl-4-yl-methanol 162-163 "C Meo
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