4. A new method for the determination of mercury in fish was tested against a N.I.S.T. standard to determine if there was any bias (determinate error) in the new technique. The N.I.S.T. standard fish sample was certified to contain 13.55 ppm Hg. The results of six analyses by the new method gave a mean value of 14.15 ppm and s.d. = 0.42 ppm. Does the new method give accurate results at the 95% confidence level?
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- StatisticalAnalysis of Data. Provide what isasked. a.Mean values of ppm Ca and ppm Mg .b.Median values of ppm Ca and ppm Mg. c.Std. dev. of ppm Ca and ppm Mg.The standard addition method is used to analyze a sample of a river water for mercury. Solution A is made by pipetting 5.00 mL of undiluted sample in to a 10 mL volumetric flask and filling to the mark with D water. Solution B is made by pipetting 5.00 mL of undiluted sample and 3.00 mL of 15.0 ppb of Hg standard into same 10.0 mL volumetric flask and filling to the mark with DI. Solution A and B are analyzed using atomic absorption spectroscopy and give a percent transmittance values of 56 % and 33 % respectively (not blank corrected). A blank has a transmittance of 96%. Which of the following technique can be used to determine the amount of mercury in the undiluted sample of river water? O A. IR spectroscopy O B. Cold vapor atomic absorption OC. Hydride generation atomic absorption OD. Electrothermal atomic absorptionThe homogeneity of the chloride level in a water sample from a lake was tested by analyzing por- tions drawn from the top and from near the bottom of the lake, with the following results in ppm CI: Top 26.30 Bottom 26.22 26.43 26.32 26.28 26.20 26.19 26.11 26.49 26.42 (a) Apply the i test at the 95% confidence level to determine if the means are different. (b) Now use the paired / test and determine whether there is a significant difference between the top and bottom values at the 95% confidence level. (c) Why is a different conclusion drawn from using the paired i test than from just pooling the data and using the normal i test for differences in means?
- The standard addition method is used to analyze a sample of a river water for mercury. Solution A is made by pipetting 5.00 mL of undiluted sample in to a 10 mL volumetric flask and filling to the mark with DI water. Solution B is made by pipetting 5.00 mL of undiluted sample and 3.00 mL of 15.0 ppb of Hg standard into same 10.0 mL volumetric flask and filling to the mark with DI. Solution A and B are analyzed using atomic absorption spectroscopy and give a percent transmittance values of 56 % and 33 % respectively (not blank corrected). A blank has a transmittance of 96%. What is the corrected absorbance of both solution A and B? A. Solution A: 0.123 Solution B: 0.463 B. Solution A: 0.463 Solution B: 0.234 C. Solution A: 0.123 Solution B: 0.234 D. Solution A: 0.234 Solution B: 0.463The standard addition method is used to analyze a sample of a river water for mercury. Solution A is made by pipetting 5.00 mL of undiluted sample in to a 10 mL volumetric flask and filling to the mark with DI water. Solution B is made by pipetting 5.00 mL of undiluted sample and 3.00 mL of 15.0 ppb of Hg standard into same 10.0 mL volumetric flask and filling to the mark with DI. Solution A and B are analyzed using atomic absorption spectroscopy and give a percent transmittance values of 56 % and 33 % respectively (not blank corrected). A blank has a transmittance of 96%. What is the corrected absorbance of both solution A and B? O A. Solution A: 0.123 Solution B: 0.463 O B. Solution A: 0.463 Solution B: 0.234 O C. Solution A: 0.123 O D. Solution A: 0.234 Solution B: 0.234 Solution B: 0.4637) The homogeneity of the chloride level in a water sample from a lake was tested by an analyst. Below are the concentration in parts per million (ppm) of Cl: 27.32, 27.22, 27.21, 27.24, 27.20 i. Determine the mean and median. ii. Calculate the confidence limit at 90%. iii. Identify a possible outlier and use the Q-test to determine whether it can be retained or rejected at 90% confidence level
- The standard addition method is used to analyze a sample of a river water for mercury. Solution A is made by pipetting 5.00 mL of undiluted sample in to a 10 mL volumetric flask and filling to the mark with DI water. Solution B is made by pipetting 5.00 mL of undiluted sample and 3.00 mL of 15.0 ppb of Hg standard into same 10.0 mL volumetric flask and filling to the mark with DI. Solution A and B are analyzed using atomic absorption spectroscopy and give a percent transmittance values of 56 % and 33 % respectively (not blank corrected). A blank has a transmittance of 96%. What is the corrected absorbance of both solution A and B? OA. Solution A: 0.123 Solution B: 0.463 O B. Solution A: 0.463 Solution B: 0.234 O C. Solution A: 0.123 Solution B: 0.234 O D. Solution A: 0.234 Solution B: 0.463Anna analyzed arsenic content on a fish purchased from local wet market. According to Food Regulation 1985, permissible level for arsenic in fish and fishery product is 1 ppm. In this study, an average of 11.4 2.1 ng/g was obtained based on six sample replicates. Suggest a suitable analytical instrument to be used in this analysis and draw a conclusion on the safety of arsenic content of this fish sample.Complete the given data sheet in determination of total alkaline strength in soda ash. Show your computations. Wt. of soda ash Vf HCI V; HCI Vf NaOH Vi NaOH %Na₂CO3 %Na₂O %Na₂CO3 = Percentage purity of sample: mLs x Ns x me. wt.xx 100 wt.sample x% 0.4 g 4.6 mL 0 mL 0 mL 0 mL | Alkaline strength of sample in terms of %Na2CO3 or %Na2O: mLs x Nsx me.wt.Na₂ox 100 wt.sample 0.4 g 10.2 mL 4.6 mL 0 mL 0 mL ||
- Calculation of the volume of 1.25 M NaOH (aq.) required to extract 1.0 gram of 2-naphthol. Use 20% mole excess of NaOH (i.e. use 1.2 mol of NaOH for every 1 mol of 2-naphthol).why is it better to generate a calibration plot than to perform a determination using a single measurements for a standard solution?1. Part A Solution temperature = 24 °C Conductivity of instrument grade water = 1.043 uScm! Conductivity of deionised water = 1.74 µScm! Conductivity of tap water = 330 μScml On the basis of data above comment on conditions of the different water grades. 2. The experimental data for electrolytes in Part B are given below: Electrolyte c (M) K (ms.cm') HC1 0.01 5.06 KCI 0.01 1.415 NaCl 0.01 1.236 CaCl2 0.01 2.30 КОН 0.01 2.29 CH3OH 0.01 0.003 K2SO4 0.01 2.65 Calculate molar conductivity A of each electrolyte solution in Sm/mol above. Correct for the conductivity of deionized water.