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- It is required to know the concentration of an aqueous solution of H2SO4 that appeared in the laboratoryChemistry III and it's unlabeled. To this end, a student of analytical chemistry carried out the followingProcedure: He took 5.00 mL of a fresh and standardized solution of 0.525M NaOH and brought them to a250.0 mL balloon to be completed with distilled water. Subsequently, he poured 15.00 mL of the solutionH2SO4 of unknown concentration in an Erlenmeyer flask and added 2 drops of phenolphthalein.Using a burette filled with the last NaOH solution, he noticed that when adding 39.40 mL of the hydroxidethe Erlenmeyer solution reached a faint but permanent pink. With the above dataDetermine the concentration and pH of the H2SO4 solution.Arsenic(III) oxide (As2O3) is available in pure form and is a useful (but carcinogenic) primary standard for oxidizing agents such as MnO4-. The As2O3 is dissolved in base and then titrated with MnO4- in acidic solution. A small amount of iodide (I - ) or iodate (IO3-) is used to catalyze the reaction between H3AsO3 and MnO4-. As2O3 + 4 OH - 2 HAsO32- + H2OHAsO32- + 2 H+ H3AsO35 H3AsO3 + 2 MnO4- + 6 H+ 5 H3AsO4 + 2 Mn2+ + 3 H2O (a) A 3.209 g aliquot of KMnO4 (FM 158.034) was dissolved in 1.000 L of water, heated to cause any reactions with impurities to occur, cooled and filtered. What is the theoretical molarity of this solution if no MnO4- was consumed by impurities? M(b) What mass of As2O3 (FM 197.84) would be just sufficient to react with 25.00 mL of the KMnO4 solution in part (a)? g(c) It was found that 0.146 8 g of As2O3 required 29.98 mL of KMnO4 solution for the faint color of unreacted MnO4- to appear. In a blank titration, 0.03 mL of MnO4- was required to produce enough…H.W 1) Calculate the number of meq. of H;C:O..2H;0 (fw= 126.1) in 0.5 gm of the pure compound assuming that two hydrogen ions to titrated with standard base? 2) A standard AGNO, solution prepared by weighting exactly 24.15 gm of carefully prepared solid, dissolving in water and diluting in a volumetric flask to exactly 2 L. What normality of the solution?
- A sample of Al;(SO.); weighing 7.52-g was dissolved in enough water and diluted to 250.0-mL. 100.0-mL of the dilution was transferred to another flask, 10.0-mL of 0.050M EDTA, 20-ml of buffer solution, 50-mL of alcohol and 2.0-ml dithizone TS were added. The resulting solution required 8.7-mL of 0.031M ZnSO, to reach the endpoint. (Note: Each ml of 0.050M EDTA is equivalent to 16.66-mg Al:(SO.);•18H;0). Compute for the percent purity of the sample.A 4.912-g sample of a petroleum product was burnedin a tube furnace, and the SO2produced was collectedin 3% H2O2.Reaction:SO2(g)+H2O2→H2SO4A 25.00-mL portion of 0.00873 M NaOH was introducedinto the solution of H2SO4, following whichthe excess base was back-titrated with 15.17 mL of0.01102 M HCl. Calculate the sulfur concentrationin the sample in parts per million.Calculate the concentration of Fe2O3 in a mineral sample after solubilization of 0.4891g and availability of Fe as Fe2+. The released Fe2+ ions were titrated with a 0.02153 mol/L K2Cr2O7 solution requiring 36.92 mL to reach the end point of the titration. Show the calculations and express the concentration in % m/m. K2Cr2O7; + 6Fe2+ + 14H+ → 2Cr+3 + 2K+ + 6Fe3+ + 7H20
- A 0.64 g sample containing KCl ( mw = 74.6 ) is dissolved in 50mL of water and titrated to the Ag2CrO4 end point, requiring 26.2 mL of 0.15 M AgNO3 .The %w/w KCl in the sample is ?A 20 mL volume of 0.015 M KIO3 containing an excess of KI, is added to a 0.312 g sample of a Real Lemon solution containing vitamin C. The Yellow-brown solution, caused by excess I2 is titrated to a colorless starch endpoint with 11.3 mL pf 0.106M Na2S2O3. Question: What is the equation for I- titrated with the IO3 standard solution.The concentration of CO in the air can be determined by passing a known volume of air through a tube containing I2O5, resulting in the formation of CO2 and I2. I2 is removed from the tube by distillation and collected in a solution containing excess KI, producing I3-. I3- is titrated with a standard solution of Na2S2O3. A 4.79 L air sample was sampled as described here, requiring 7.17 ml of 0.00329 M Na2S2O3 to reach the endpoint in a typical analysis. If the density of the air is 1.23×10^-3 g/ml, what is the amount of CO in the air in ppm? (CO: 28 g/ml)
- The E0 for the reaction Pb3(AsO4)2 (s) + 6e- ⇆ 3Pb(s) + 2AsO43- is -0.475 V. Calculate the solubility product constant for Pb3(AsO4)2 ?Pb2 + + 2e- ⇆ Pb(s) E0=-0.126 V1. A 0.4515-g sample of solid containing a mixture of only CuSO4 5H2O and Hg(NO:)2 required 29.52 mL of 0.1133 M KSCN to complete titration of both metals. Write balanced net ionic equations for the reactions of each metal with the titrant. Calculate the wt% of Hg in the solid sample.For Redox Analysis of Iron... ~0.02 M of potassium dichromate is prepared as titrant for dried unknown. ~.3 g of sample, 50ml of 6M HCl, 20mL SnCl2, 10 mL of saturated HgCl2 solution, 60 mL of 3M H2SO4, 15mL of concentrated H3PO4, 100mL DI water. HCl (+ heat in fumehood until samples dissolves), SnCl2 (added with pipet until solution changes from yellow to colorless/light green with 3 drops in excess), HgCl2 (after cooling), H2SO4, H3PO4, DI Water, is added to the sample solution with 8 drops of diphenylamine sulfonate indicator then titrated with the potassium dichromate to a violet blue endpoint. 3. How would you prepare a complete anlaysis procedure using KMnO4 as the oxidant instead of K2CrO7? Include sample and solution preparation, approximate weights of samples and reagents, procedure and chemical reactions. In particular what is the purpose of the Zimmerman Reinhardt Reagent?